Crystal structure of catena-bis[2,2'-(1,3-propanedithio)- bis(1,3,4-thiadiazole)]bis(2,4,6-trinitrophenolate)copper(II), Cu(C7H8N4S4)2(C6H2N3O7)2

Jian-Hua Qin, Ai-Qin Tian, Jian-Ge Wang, Pu-Zhou Hu
2011 Zeitschrift für Kristallographie - New Crystal Structures  
C 26 H 20 CuN 14 O 14 S 8 ,triclinic, P1 (no. 2), a =8.709(1 Source of material The reaction of 2,2'-(1,3-propanedithio)bis(1,3,4-thiadiazole) (0.1 mmol) with copper dipicrate tetrahydrate (0.1 mmol) in MeOH (10 mL)f or af ew minutes afforded al ight blue solid, which was filtered, washed with acetone, and dried in air. The single crystals suitable for X-ray analysis were obtained by slow diffusionofEt 2 Ointothe acetonitrile solution of thesolid.
doi:10.1524/ncrs.2011.0208 fatcat:urn2vkq2lfgofn4p6ijkny2xii