Crystal structure of a diaqua-bis(3,5-di(1H-imidazol-1-yl)pyridine-κN)-bis(2-(4-carboxy-phenyl)acetato-κO]manganese(II), C40H36MnN10O10

Feng-Yang Ju, Wen-Bo Guo, Yun-Ping Li
2017 Zeitschrift für Kristallographie - New Crystal Structures  
C 40 H 36 MnN 10 O 10 , monoclinic, P21/c (no. 14), a = 21.8966(12) Å, b = 7.2586(4) Å, c = 12.2346(6) Å, β = 98.232(1)°, V = 1924.52(18) Å 3 , Z = 2, Rgt(F) = 0.0327, wR ref (F 2 ) = 0.0847, T = 296(2) K. CCDC no.: 1536054 The centrosymmetric title complex is shown in the figure (carbon-bound hydrogen atoms are omitted for clarity). Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters.
more » ... ment parameters. Source of material A mixture of 3,5-bis(1-imidazoly)pyridine (bip, 0.05 mmol, 45 mg), 4-carboxybenzeneacetic acid (H 2 cbaa, 0.05 mmol, 9.0 mg), Mn(OAc) 2 ×4H 2 O (0.1 mmol, 24 mg), ethanol
doi:10.1515/ncrs-2016-0288 fatcat:dtj2zauqcffoxdr7fgn65fw7ta