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Described herein is a novel route to 2-phenylindoxyls. A previously undisclosed acid catalyzed reaction of N-hydroxyalkyl-3-acetoxy-2-phenylindoles gave the desired 2-phenylindoxyls, the identity of which was confirmed by 2D-NMR. The product structure represents a scaffold that could be exploited in a pharmaceutical or academic setting.doi:10.3998/ark.5550190.0007.b03 fatcat:afry6jdrsvdytejli5ty4dztcu