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C 18 H 24 CoN 10 O 2 S 4 ,monoclinic, P2 1 /n (no. 14), a =8.021(1) Å, b =16.120(2) Å, c =10.480 (2) Source of material An aqueoussolution(5mL) of cobalt sulphate (1 mmol, 0.250 g) was slowly poured dropwise into ahot aqueous solution (3 ml) of ammonium thiocyanate (1 mmol, 0.0761 g). The mixture was stirred for 10 mins. 2,2'-Biimidazole (H 2 biim,1mmol, 0.134 g) and DMSO (4 ml)were added to this mixture. The resultant mixture was refluxed for 30 min and then allowed to cool to ambientdoi:10.1524/ncrs.2011.0280 fatcat:xmtmmsofkzctfd5ku3tt33qgya