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1-(2-pyridylazo)-2-naphthol; Benzotriazole; Voltammetry; Rotating disc electrode (RDE). KEYWORDS ABSTRACT Electrochemical investigations of 1,2,4-triazole and benzotriazole in aque-ous acidic media has been carried out by cyclic voltammetric measurements. Cyclic voltammetric experiments were carried on glassy carbon (GC) working electrode. Effect of potential scan rate, pH of the solution and use of different surfactant on the electrochemical behavior has been investigated. Single reductionfatcat:weicgdb5r5e7dcyilvuw4jdzrm