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Here, we adapt the catalytically self-threading polyrotaxane synthesis for the construction of two-dimensional polymeric thin films using a water−oil interfacial polymerization method. In this method, the polymerization and the rotaxane formation take place simultaneously at the interface because of the presence of catalytically active cucurbituril (CB6) that can facilitate 1,3-dipolar cycloaddition reaction between alkyne and azide to form polytriazoles. By varying the concentration of thedoi:10.1021/acsapm.0c01010.s001 fatcat:2hkol7up5rbpfexnlp7raermvm