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Tetra-tert-Butyl-di-m-Hydroxo Digallium(III) and 1,12-Diaza-3,4:9,10-Dibenzo-5,8-Dioxo-cyclo-Pentadecane. Structure and Isomers of the Coordination Compound
International Journal of Molecular Sciences
Tri-t-butylgallium has been reacted with the macrocycle 1,12-diaza-3,4:9,10dibenzo-5,8-dioxocyclopentadecane which could be a potential ligand for gallium(III). A reaction product was analyzed and single crystal X-ray diffraction experiments showed that it consisted of the cyclic dimer of di-t-butylgallium-hydroxide hydrogen bonded to the macrocycle. Without a co-crystallized organic molecule di-t-butylgallium hydroxide crystallizes as a trimer. Density functional calculations have been used todoi:10.3390/i6110276 fatcat:5hfokg2nprdtvfg3fdrkyccem4