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Crystal structure of η6 -benzene(chloro)(N-[(5)-(-)1-phenylethyl]-thiobenzamidato)ruthenium(II), (C6H6)Ru(C15H14NS)Cl
2002
Zeitschrift für Kristallographie - New Crystal Structures
C21H20CINR11S, orthorhombic, P2i2& (No. 19), a = 11.8187(5) Â, b = 16.1775(6) Â, c = 29.993(1) Â, V= 5734.5 Â 3 , Z= 12, R gl (F) = 0.037, wR^F 2 ) = 0.067, T= 173 K. Source of material 483 mg (2.00 mmol) of ^-[(5)-(-)l-phenylethyl]thiobenzamide [1, 2] were dissolved in CH2CI2 (20 ml) and cooled to 223 Κ [(?7 6 -benzene)RuCl2]2 (500 mg, 1.00 mmol) was added at this temperature. After stirring the mixture for 16 h while raising the temperature to r.t. the dark red solution was filtered through
doi:10.1524/ncrs.2002.217.jg.551
fatcat:actk4cwiivez5eifjzlgpfenzq