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Examination of the cation-exchange capacity of a hydrated halloysite from Djebel Debar has disclosed no evidence for the proposed existence of exchangeable interlayer ions. A series of labile halloysite-salt complexes has been prepared. The requirements for effective intercalation of the salt are a high salt concentration in the external solution phase and a cation of low hydration energy.doi:10.1180/claymin.1959.004.22.02 fatcat:3oaop5n3prhzdfiwwx4jsmjn3a