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Sample of Ni1-xCuxFe2O4where (x=0.05, 0.10, 0.15) has been prepared by root equation method. X-ray diffraction and K-absorption fine structural measurements have been carried out. The sample structure has been found to be cubic. X-ray diffraction measurements have been used to determine particle size and lattice parameter. EXAFS spectra has been recorded at 2.5Gev Indus -2 Synchrotron radiation source at RRCAT, Indore, India. EXAFS data have been analysed by computer software Athena.doi:10.1088/1742-6596/836/1/012042 fatcat:mqi32u7jrreshg6vugftljesou