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Determination of Aldehydes in Diatoms by Headspace Solid-Phase Microextraction Coupled with GC-MS
Journal of Chromatographic Science
Reactive unsaturated aldehydes produced by marine diatoms upon cell damaged interfere negatively with the reproduction success of their grazers. In this paper, a method based on headspace solidphase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS) was developed for analysis of six aldehydes: [(E)-2-hexenal, heptanal, (E)-2-heptenal, (E,E)-2,4-heptadienal, (E)-2-decenal, (E,E)-2,4-decadienal] in two laboratory cultured diatoms (Skeletonema costatum anddoi:10.1093/chrsci/49.1.15 fatcat:ysawk2odu5ctjng5aqe5xxmjpi