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Mechanochemistry offers sustainable synthesis of the functionalized cellulose nanofiber (CNF). In this study, changes in the microstructure of the CNF aqueous sol by planetary ball milling were investigated in terms of its rheological behavior, crystallinity, and diameter distribution. The surface activity of the CNF was additionally characterized by a pulsed nuclear magnetic resonance (NMR). A decreased thixotropy hysteresis loop observed in the 100 min −1 -treated CNFs indicated a weakerdoi:10.4164/sptj.58.164 fatcat:34qzcpxwhjgdpjto54d4bxyige