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Superconductive rhenium films were electrodeposited from a water-in-salt type electrolyte with superhigh concentration of LiCl. Rhenium free electrolytes were also studied with linear sweep voltammetry to further understand the effects of LiCl salt concentration on the ion activity and side reactions. The morphology, crystallographic structures and superconductivity of the electrodeposited Re films were characterized. The hydration of LiCl resulted in a depletion of free water molecules and adoi:10.1149/2.0261816jes fatcat:556o562grrglhmdladlnroz72u