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Transition metal complexes with thiosemicarbazide-based ligands, Part 58. Synthesis, spectral and structural characterization of dioxovanadium(V) complexes with salicylaldehyde thiosemicarbazone
2011
Journal of the Serbian Chemical Society
The first two complexes of dioxovanadium(V) with salicylaldehyde thiosemicarbazone (SALTSC), of the coordination formulas [VO 2 (SALTSC--H)]·H 2 O (1) and NH 4 [VO 2 (SALTSC-2H] (2), were synthesized and characterized by elemental analysis, conductometric measurements, IR and UV-Vis spectroscopy and X-ray analysis. The complexes were obtained in the reaction of an aqueous ammoniacal solution of NH 4 VO 3 and SALTSC. The results of the characterization showed that SALTSC was coordinated in the
doi:10.2298/jsc101217078v
fatcat:4qy33467gvaszga4ic5ke3ukwi