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C4H 3 IN4O4, orthorhombic, Pbca (no. 61), a = 9.9513(6) Å, b = 11.3365(4) Å, c = 14.3295(12) Å, V = 1616.55(17) Å 3 , Z = 8, Rgt(F) = 0.0279, wR ref (F 2 ) = 0.0684, T = 105.6 K. CCDC no.: 1520552 The asymmetric unit of the title crystal structure is shown in the gure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of material The title compound was prepared by nitrifyingdoi:10.1515/ncrs-2016-0209 fatcat:mq37jdmiqjgc7lvywvh347in5e