The crystal structure of 1-methyl-2,4-dinitro-5-iodoimidazole, C4H3IN4O4

Chen Lizhen, Lian Pengbao, Wang Jianlong
2017 Zeitschrift für Kristallographie - New Crystal Structures  
C4H 3 IN4O4, orthorhombic, Pbca (no. 61), a = 9.9513(6) Å, b = 11.3365(4) Å, c = 14.3295(12) Å, V = 1616.55(17) Å 3 , Z = 8, Rgt(F) = 0.0279, wR ref (F 2 ) = 0.0684, T = 105.6 K. CCDC no.: 1520552 The asymmetric unit of the title crystal structure is shown in the gure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of material The title compound was prepared by nitrifying
more » ... d by nitrifying 1-menthyl-2,4,5-triiodoimidazole. It was recrystallized from acetone solution at room temperature to give colorless crystals suitable for single-crystal X-ray di raction.
doi:10.1515/ncrs-2016-0209 fatcat:mq37jdmiqjgc7lvywvh347in5e