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Nanocrystalline yttria-stabilized zirconia powders, synthesized by the citrate nitrate gel combustion route, with yttria concentration varying from 8 to 12 mol% were studied by in situ high temperature X-ray diffraction in the temperature range of 25–1000°C. The sample obtained has a high specific surface area of 35 m2/g while calculated surface area was around 123 m2/g. The in situ high temperature X-ray diffraction study revealed that crystallite size remains in the range of 7–9 nm up todoi:10.5402/2011/305687 fatcat:knynukto25dbje6jfnjelu5sf4