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Pure CeO 2 and 20 mol. % Cu/CeO 2 composite nanofibers were fabricated by using Electrospinning method. Copper acetate monohydrate and cerium nitrate hexahydrate were used as the inorganic precursors, PVP was used as the guiding polymer and the electrospinning was carried out at 12kV DC voltage by maintaining a tip to collector distance of 10 cm. The synthesized nanofibers were characterized by SEM and EDX analysis and the average diameters of pure ceria and 20 mol. % Cu/CeO 2 nanofibers werefatcat:lbrg5byuinhh3izticqb27g2je