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In the present research, Microwave Assisted Synthesis(MAS) method is applied to synthesize high performance titania(TiO 2) at 150 o C with various heating time. Each prepared titania are characterized by SEM, XRD and N 2 sorption analysis(BET and BJH calculation). This study has shown that the prepared titania by MAS method heated at 150 o C with 4 hours treatment has the highest photocatalytic performance compared to the commercial TiO 2 and others titania described in this paper. The titaniafatcat:dueo2uyn6nb3pd3atsyw437rf4