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The site-distributions of Fe in four BZordered NiAl-based alloys with Fe concentrations of 10% 2%, and 0.5% have been determined by ALCHEMI (atom-location by channeling-enhanced microanalysis). Site-distributions have been extracted with standard errors between -1.5% (10% Fe concentration) and -6% (0.5% Fe concentration). The results show that Fe has no strong sitepreference in NiAl and tends to reside on the site of the stoichiometrically deficient host element. An improved ALCHEMI analysisdoi:10.1557/proc-364-443 fatcat:6babshzidzhydkt4twjmohqh7m