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This thesis details the characterisation of lipophilic cation radiotracers for biomedical imaging. The radiotracers discussed are based on triphenylphosphonium cations which can accumulate in the mitochondria and are radiolabelled with either [18F] or [11C]. Implementation of existing radiotracers and development of novel [11C] based di- phosphonium di-cation radiotracers is described in Chapter 3. The chemistry required to produce precursors, reference compounds and radiolabelling is discusseddoi:10.25560/68030 fatcat:j5x3g5zvcjf7jniji6wb4q3yzy