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A potentiometric technique based on surfactant ion selective electrode has been used for various cationic and anionic surfactants. The data obtained contain m 1 (surfactant monomer concentration); m 2 (free counterion concentration) and (degree of dissociation of micelle) were used for determination of aggregation number at and above cmc (critical micelle concentration). Data fitting show a relationship between aggregation number with such parameters. The correlation equation obtained showsdoi:10.1080/0031910021000044438 fatcat:ujq4r4qhkne3xmavtnkeyzx5ey