Crystal structure of trans-9-thiabicyclo[6.1.0]nonan-3-ol, C8H13(S)OH

K. Peters, E.-M. Peters, B. Fröhling, S. Weinkötz, W. Adam
1999 Zeitschrift für Kristallographie - New Crystal Structures  
CgHuOS, monoclinic, C12/cl (No. 15 ), a = 20.631(7) Ä, b = 7.016(2) Ä, c = 23.813(7) Ä, β = 93.32(2)°, V = 3441.1 Ä 3 , Z= 16, Rg{F) = 0.082, R^F) = 0.075, T= 293 K. Source of material The title compound was prepared according to [1], The crystal decomposed within about 26 h during the measurement. Discussion Due to the hydrogen bond ΟΙ-ΗΙΟΓ four molecules form an approximate tetragonal four-membered isolated cluster.
doi:10.1515/ncrs-1999-0263 fatcat:fo42a4bpzrcijcef7anvcecjya