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Photocatalytic oxidation of mono- and di-substituted arylboronic acids to phenols has been investigated in a continuous flow LED photoreactor. In EtOH–H2O, conversion was accelerated at 2 MPa; whereas reactions at 0.1 MPa led to 64% desymmetrisation.doi:10.1039/c4ra15588b fatcat:fehekofusjcg3gmtzmkoxc2bbi