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Ternary Ni-P-Al alloy coating was fabricated by magnetron sputtering technique with a Ni-P/Al composite target source. The effects of thermal treatments, including deposition process heating and postannealing, on phase transformation phenomenon and related mechanical properties were investigated. The as-deposited coatings produced under process temperature below showed an amorphous/nanocrystalline microstructure. Significant crystallization of Ni matrix and precipitation of and compounds weredoi:10.1155/2011/802093 fatcat:dkruj3roxbghjbvcohtds6h55m