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In this novel paper, we synthesized binuclear complexes of metal chloride of Cu(II), Ni(II) with organic compounds 3,3'-dihydroxy benzidiene and 2-amino thiophenol. The type of complex is [LM 2 Cl 4 ]. The characterization had been found from elemental analysis, molar conductivity, Infrared, Ultraviolet-visible, cyclic voltammetry, TG-DTA, magnetic measurements, DNA cleavage study and antimicrobial study. The elemental analysis suggested that the metal-ligand ratio is 2:1. The microbesdoi:10.31788/rjc.2020.1315538 fatcat:scve43irb5ffdljyyturd2s5hy