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Crystal structure of bis(1,10-phenanthroline-N,N′)bis(4-fluorobenzoato- O,O′)tetrakis(μ-4-fluorobenzoato-O,O′)didysprosium(III), Dy2(C6H4FCOO)6(C12H8N2)2
2006
Zeitschrift für Kristallographie - New Crystal Structures
C 66H40Dy2F6N4O12, triclinic, P1 (no. 2), a = 9.915(1) Å, b = 11.775(1) Å, c = 14.775(2) Å, a = 106.704(2)°, b = 107.835(2)°, g = 101.476(2)°, V = 1493.0 Å Source of material 1.05 mmol 4-fluorobenzoic acid were dissolved in 7 ml distilled water by dropping 2 M NaOH solution and the pH of the solution was adjusted to 5-6. Then 0.35 mmol 1,10-phenanthroline (phen) and 0.35 mmol DyCl 3 • 6H2O were added to the solution successively. The mixture was placed in 25 ml Teflon-lined reactor and heated
doi:10.1524/ncrs.2006.221.1.7
fatcat:ljbxhshye5fdpokqdzfcwhekmm