Internet Archive Scholar

Crystal structure of dichloro((S)-2-(anilinomethyl)-pyrrolidine)- palladium(II), Pd(Cl)2(C11H16N2)

Larbi El Firdoussi, Mustapha Ait Ali, Abdallah Karim, Anke Spannenberg
2007 Zeitschrift für Kristallographie - New Crystal Structures  

Preserved Fulltext

fulltext thumbnail
Web Archive Capture PDF (147.2 kB)
https://web.archive.org/web/20180727121836/https://www.degruyter.com/downloadpdf/j/ncrs.2007.222.issue-3/ncrs.2007.0080/ncrs.2007.0080.pdf

A copy of this work was available on the public web and has been preserved in the Wayback Machine. The capture dates from 2018; you can also visit the original URL. The file type is application/pdf.

C 11H 16Cl 2 N 2 Pd, orthorhombic, P 2 1 2 1 2 1 (no. 19), a =11.246(2) Å, b =12.222(2) Å, c =19.637(4) Å, Source of material The title compound was preparedbyreaction of Li 2 PdCl 4 and ( S )-2-(anilinomethyl)-pyrrolidine (molar ratio 1:1) in distilled water at 298 K.The resulting yellow solid, after concentration to dryness, was treated with am ixture of CH 2 Cl 2 /CH 3 OH.After filtration from the resulting solution, crystals of the complex were obtained. Experimental details All
more » ... atoms, except the disordered Catoms which were refined only isotropically, were refined anisotropically. The Hatoms bound to Catoms were included at calculated positions and refined by using the riding model. The Hatoms attached to N atoms were found from Fourier difference maps and refined freely.
doi:10.1524/ncrs.2007.0080 fatcat:atugvwkpyvclthpgp4ickqill4
DOAJ
Citation

Larbi El Firdoussi, Mustapha Ait Ali, Abdallah Karim, Anke Spannenberg. "Crystal structure of dichloro((S)-2-(anilinomethyl)-pyrrolidine)- palladium(II), Pd(Cl)2(C11H16N2)." Zeitschrift für Kristallographie - New Crystal Structures 222.3 (2007)