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Progress is reported on the development of analytical methods for the determination of uranium and plutonium for nuclear safeguards application and the preparation of well-characterized plutonium-containing materials.for laboratory evaluation purposes and as standards. A Teflon-container, metal-bomb apparatus has been developed for the dissolution of samples in acids, including hydrofluoric acid, at temperatures to 280°C and pressures to 5000 psi.doi:10.2172/4607774 fatcat:hx4iikmx6bhetk66y6zqqj6ilm