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In this work, the metal organic frameworks (MOFs) Cu-bipy-BTC ([Cu2(OH)(2,2'-bipy)2(BTC)3 2H2O]n) were in situ synthesized on the surface of a gold electrode directly to form a hybrid material of a Cu(OH)2 nanosheet and Cu-bipy-BTC nanoparticle. The structure of this hybrid material on the electrode surface was characterized using Fourier-transform infrared spectroscopy, X-ray diffraction, scanning electron microscopy, and energy-dispersive spectrocopy. It is shown that the newly in situdoi:10.20964/2020.08.52 fatcat:c37wkyo4nra3xb3mz6ikpgqiqe