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α -LiFeO2 has been synthesized using Fe2O3 and LiNO3 under various conditions, and the relationship between the CO2 absorption ability and structural phase transition of the synthesized α -LiFeO2 has been investigated by X-ray diffraction (XRD) analysis and thermogravimetry and differential thermal analysis (TG-DTA). Mixed powders of Fe2O3 and LiNO3 were heated at 500°C for 5 h to synthesize α -LiFeO2. The CO2 absorption reaction of the synthesized α -LiFeO2 was performed in the temperaturedoi:10.2109/jcersj2.118.48 fatcat:2clyfcrtknhtjo3ap33thqwwq4