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Solid-state 29Si NMR and FTIR analyses of lignin-silica coprecipitates
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by
Yohanna Cabrera Orozco,
Andrés Cabrera,
Flemming Hofmann Larsen,
Claus Felby
Abstract
<jats:title>Abstract</jats:title>When agricultural residues are processed to ethanol, lignin and silica are some of the main byproducts. Separation of these two products is difficult and the chemical interactions between lignin and silica are not well described. In the present study, the effect of lignin-silica complexing has been investigated by characterizing lignin and silica coprecipitates by FTIR and solid state NMR. Silica particles were coprecipitated with three different lignins, three lignin model compounds, and two silanes representing silica-in-lignin model compounds. Comparison of
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