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Spectroelectrochemical Study of Neptunium in Molten LiCl-KCl Eutectic
release_eq6ezfr5ajgopmpg75zyjtcnly
by
Ilya B. Polovov,
Clint A. Sharrad,
Iain May,
Vladimir A. Volkovich,
Boris D. Vasin
Published
in Zeitschrift fur Naturforschung A-A Journal of Physical Sciences
by Walter de Gruyter GmbH.
2007 Volume 62, Issue 12
Abstract
Neptunium behaviour in an LiCl-KCl eutectic melt at 723 K was studied using spectroelectrochemistry. Cathodic reduction of neptunium(IV)-containing melts led to the formation of Np(III) ions and then neptunium metal. Electronic absorption spectra of Np(IV) and Np(III) chloro species in LiCl-KCl melt were recorded and resolved into individual Gaussian bands. The nature of neptunium complex ions in the melt is discussed.
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