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Schwingungsspektren von Überjodsäuren und Perjodaten, I./Vibrational Spectra of Periodic Acid and Periodates, I
release_3qjm4spwwjfcvpltmxirkqebki
by
Hans Siebert,
Gertraud Wieghardt
Published
in Zeitschrift für Naturforschung. B, A journal of chemical sciences
by Walter de Gruyter GmbH.
1972 Volume 27, Issue 11, p1299-1304
Abstract
The vibrational spectra of H<jats:sub>5</jats:sub>IO<jats:sub>6</jats:sub> and a number of periodates containing the anion IO<jats:sub>6</jats:sub><jats:sup>5-</jats:sup> are reported and frequencies are assigned. The force constants of the IO<jats:sub>6</jats:sub><jats:sup>5-</jats:sup> ion are interpreted on the basis of noticeable π bonding. The IO bonds in H<jats:sub>5</jats:sub>IO<jats:sub>6</jats:sub> are not all equivalent. As shown by their Raman spectra, solutions of H<jats:sub>5</jats:sub>IO<jats:sub>6</jats:sub> in concentrated strong acids contain the hexahydroxoiodine(VII) ion I (OH)<jats:sub>6</jats:sub><jats:sup>+</jats:sup> with six equivalent IO bonds.
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